20.500.12556/DKUM-41338 Koordinacijske spojine cinkovih acetatov s piridinkarboksamidi Coordination compounds of zinc acetates with pyridinecarboxamides Namen diplomske naloge je bil sinteza novih cinkovih koordinacijskih spojin iz cinkovega(II) acetata dihidrata in piridinkarboksamidov (izonikotinamid, nikotinamid in pikolinamid). Najprej smo sintetizirali cinkov(II) hidroksid, ki smo ga potem uporabili za sintezo cinkovega(II) acetata dihidrata. Izvajali smo reakcije med cinkovim(II) acetatom dihidratom in piridinkarboksamidi. Sintetizirane kristale smo karakterizirali z rentgensko praškovno difrakcijo, termogravimetrično analizo in Fourierjevo transformacijsko infrardečo spektroskopijo. Moje delo je bilo namenjeno sintezi in karakterizaciji novih koordinacijskih spojin. The purpose of this diploma work was to synthesize new zinc coordination compounds out of zinc(II) acetate dihydrate and pyridinecarboxamides (isonicotinamide, nicotinamide and picolinamide). First we synthesized zinc(II) hydroxide, which was further on used to synthesize zinc(II) acetate dihydrate. We carried out the reaction between zinc(II) acetate dihydrate and pyridinecarboxamide. The synthesized crystals were characterised with X-ray powder diffraction (XRD), thermogravimetric analysis (TGA) and Fourier transform infrared spectroscopy (FTIR). My work was devoted to the synthesis and characterization of new coordination compounds. Cinkov(II) acetat dihidrat koordinacijske spojine piridinkarboksamidi (nikotinamid izonikotinamid pikolinamid) termogravimetrična analiza (TGA) rentgenska praškovna difrakcija (RPD) Fourierjeva transformacijska infrardeča spektroskopija (FTIR). Zinc(II) acetate dihydrate Coordination compounds Pyridinecarboxamides Thermogravimetric analysis (TGA) X-ray powder diffraction (XRD) Fourier transform infrared spectroscopy (FTIR). true true false [T. Radić] Slovenski jezik Angleški jezik Diplomsko delo 2013-08-22 15:27:49 2013-09-19 10:45:06 2022-05-04 03:07:18 2021-04-25 03:09:57 2013 0 Maribor 0 0000-00-00 NiDoloceno NiDoloceno NiDoloceno 0000-00-00 0000-00-00 0000-00-00 54(043.2) 20054536 URN:SI:UM:DK:UF6KVF4Y UNI_Radic_Tanja_2013.pdf UNI_Radic_Tanja_2013.pdf 1 CAD7129350CCFA42119C0249F10285A7 543a35f6531f9f0bde65a0ac45a3c3309dc993caa416396a3a53702d74180024 26eddf08-7c0a-11eb-bb7a-00155d0001ca https://dk.um.si/Dokument.php?lang=slv&id=57107 Fakulteta za naravoslovje in matematiko 0 0 0