20.500.12556/DKUM-41867 SINTEZA BAKROVIH, NIKLJEVIH IN KOBALTOVIH KOORDINACIJSKIH SPOJIN Z NIKOTINSKO, IZONIKOTINSKO IN PIKOLINSKO KISLINO SYNTHESIS OF COPPER, NICKEL AND COBALT COORDINATION COMPOUNDS WITH NICOTINIC, ISONICOTINIC AND PICOLINIC ACID Koordinacijske spojine so dandanes pogosto sintetizirane in imajo širok spekter uporabnosti. Namen raziskave je bil sintetizirati nove in že znane koordinacijske spojine z bakrom, kobaltom in nikljem. V sklopu diplomskega dela smo izvedli 27 reakcij sinteze koordinacijskih spojin z bakrom, kobaltom in nikljem ter ligandi nikotinsko, izonikotinsko in pikolinsko kislino. Kot topila smo uporabili vodo, N,N-dimetilformamid in mešanico metanola in acetonitrila. Produkte sintez smo nato analizirali z rentgensko praškovno difrakcijo in termogravimetrično analizo. Coordination compounds are nowadays often synthesized and have a wide range of uses. The purpose of this study was to synthesize new and already known coordination compounds with copper, cobalt and nickel. As part of the thesis we performed 27 synthesis of coordination compounds with copper, cobalt, nickel and Iigands nicotinic, isonicotinic and picolinic acid. As solvents, we used water, N, N-Dimethylformamide, and a mixture of methanol and acetonitrile. Synthesis products were analyzed by X-ray diffraction and thermogravimetric analysis. koordinacijske spojine kobalt baker nikelj nikotinska kislina izonikotinska kislina pikolinska kislina rentgenska praškovna difrakcija termogravimetrična analiza (TGA) coordination compounds cobalt copper nickel nicotinic acid isonicotinic acid picolinic acid X-ray diffraction (XRD) thermogravimetric analysis (TGA) true true false [L. Goljat] Slovenski jezik Angleški jezik Diplomsko delo 2013-09-06 08:49:01 2013-09-26 13:59:19 2022-05-05 03:08:48 2021-04-25 03:33:53 2013 0 Maribor 0 0000-00-00 NiDoloceno NiDoloceno NiDoloceno 0000-00-00 0000-00-00 0000-00-00 56.562.022:543.427(043.2) 17486870 URN:SI:UM:DK:9B6YEYWK UNI_Goljat_Leja_2013.pdf UNI_Goljat_Leja_2013.pdf 1 648526FA4DA9A1581237BA78B1FDC0F3 74d02c3e220ce94786739be585baa9070f9f4e3010aee85a499da067201ba90c 6234df06-7c0a-11eb-bb7a-00155d0001ca https://dk.um.si/Dokument.php?lang=slv&id=59205 Fakulteta za kemijo in kemijsko tehnologijo 0 0 0