20.500.12556/DKUM-44300 Učinek fizikalno-kemijskih parametrov na rezultate emisijskih meritev. The influence of physico-chemical parameters on the results of emissions measurements. Diplomsko delo opisuje učinek fizikalno-kemijskih meritev analitov ter podrobno študijo vplivov posameznih parametrov na rezultate emisijskih meritev. Merilne postopke je potrebno v skladu z zahtevami standardov validirati in s tem potrditi njihovo pravilnost oziroma veljavnost. V študijo je vključena ocena merilne negotovosti in rezultati so podani v obliki validacije merilnega postopka, ki je nujna za bodočo akreditacijo metode v podjetju, kjer so bile meritve opravljene. V diplomskem delu je zajeta predstavitev emisij v zrak, trenutna zakonodaja, učinek na zdravje ljudi in način analiznega merjenja emisij. Cilj diplomske naloge je ugotoviti ustreznost merjenja emisij, kako vplivajo posamezni parametri na izvedbo meritev, rezultate in postopke izvajanja. Pomemben del predstavlja gravimetrično določanje mase filtrov, ki je potrebno pred in po zajemanju emisijkih meritev. Poseben poudarek je na presoji učinka določenih parametrov s terenskih meritev, ki so bile izvedene na objektu Ekosistemi d.o.o. Ugotovili smo, da ima vsak posamezen parameter določen vpliv na izmerjene vrednosti. Učinek vsakega parametra na merilni rezultat se povečuje z intenziteto izbrane spremembe. This thesis describes the effect of physicochemical measurements of analytes, and a detailed study of the effects of various parameters on the results of emission measurements. Measurement procedures have to be, in accordance with the requirements of the standards, validated in order to confirm their accuracy and validity. The study includes an evaluation of measurement uncertainty and the results are given in the form of validation of the measurement process, which is necessary for future accreditation of the method in a business where the measurements were made. This thesis covers the presentation of emissions into the air, current legislation, effects on human health and the analytical way of measuring emissions. The aim of the thesis is to determine the adequacy of emission measurements, how they affect the individual parameters of measurements, results and implementing procedures. An important part of the thesis presents the gravimetric determination of the mass filters, which is necessary before and after capturing the emission measurements. The thesis focused on assessing the impact of certain parameters from fieldwork measurements, which were performed at the facility Ekosistemi d.o.o. We have found that each parameter has a degree of influence on the measured value. The effect of a specific parameter on the measured result increases with the intensity of selected changes. zrak emisije merilna negotovost validacija varnost air emissions measuring uncertainty validation security true true false [R. Rudolf] Slovenski jezik Angleški jezik Diplomsko delo/naloga 2014-05-15 08:15:50 2014-05-23 08:07:34 2022-05-12 03:07:40 2021-05-01 03:15:50 2014 0 Maribor 0 0000-00-00 NiDoloceno NiDoloceno NiDoloceno 0000-00-00 0000-00-00 0000-00-00 543.423:546.217(043.2) 17859094 URN:SI:UM:DK:MNPUK0UE VS_Rudolf_Robert_2014.pdf VS_Rudolf_Robert_2014.pdf 1 824B496BA69216B31159CC42A6296643 ce5d32702747312252eba5c1d45007e68b73220444dcf0545cc1ea491bba4c0f d35c3835-7c0a-11eb-bb7a-00155d0001ca https://dk.um.si/Dokument.php?lang=slv&id=63550 Fakulteta za kemijo in kemijsko tehnologijo 0 0 0