20.500.12556/DKUM-46150 TERMIČNA ANALIZA ACETILACETONATOV PREHODNIH KOVIN Z IDENTIFIKACIJO INTERMEDIATOV THERMAL ANALYSIS OF ACETYLACETONATES OF TRANSITION METALS WITH THE CHARACTERIZATION OF INTERMEDIATES Namen diplomskega dela je bil preučiti pogoje termičnega razpada acetilacetonatov in karakterizirati intermediate, ki pri tem nastanejo. V sklopu diplomskega dela smo vzorce najprej analizirali s pomočjo termogravimetrične analize (TGA), nato pa poskušali indetificirati nastale intermediate z uporabo rentgenske praškovne difrakcije (XRD). Delo je bilo namenjeno spoznavanju termogravimetrične analize in rentgenske praškovne difrakcije. The intent of this thesis is to study conditions of the thermal decomposition of acetylacetonates and characterise intermediates which result from such process. With the help of a thermogravimetric analysis (TGA) we have analysed the samples and tried to identify created intermediates with the use of X-ray powder diffraction (XRD). In brief, the purpose of the thesis was to learn about thermogravimetric analysis and powder diffraction. acetilacetonati termična analiza barijev acetilacetonat manganov acetilacetonat železov acetilacetonat cinkov acetilacetonat bakrov acetilacetonat acetylacetonates thermal analysis barium acetylacetonate manganese acetylacetonate iron acetylacetonate zinc acetylacetonate copper aceylacetonate true true false M. Štefko] Slovenski jezik Angleški jezik Diplomsko delo/naloga 2014-09-15 02:34:44 2014-09-22 19:56:27 2022-05-17 03:10:34 2021-05-02 03:31:09 2014 0 Maribor 0 0000-00-00 NiDoloceno NiDoloceno NiDoloceno 0000-00-00 0000-00-00 0000-00-00 544.431.24:546(043.2) 18217750 URN:SI:UM:DK:791CSOEU UNI_Stefko_Martina_2014.pdf UNI_Stefko_Martina_2014.pdf 1 5431881D6B413EF1BADA72D8E63C5150 61850cbf87fe51e89e7a5ff28ed4be9b6cfe00324673d090f2ad5c37b7300e06 3d1dda19-7c0b-11eb-bb7a-00155d0001ca https://dk.um.si/Dokument.php?lang=slv&id=67293 Fakulteta za kemijo in kemijsko tehnologijo 0 0 0