20.500.12556/DKUM-54078 UPORABA SONOKEMIJSKE METODE V SINTEZI BAKROVIH METANOATOV APPLICATION OF SONOCHEMICAL METHOD IN THE SYNTHESIS OF COPPER METANOATES Sonokemija je področje kemije, kjer kemijske reakcije potekajo pod vplivom zvočne energije, imenovane ultrazvok. Ukvarja se z razumevanjem učinka zvočnih valov na kemijske sisteme. Namen naše diplomske naloge je bil sintetizirati različne modifikacije bakrovih metanoatov z uporabo klasičnih metod kot tudi z metodami sonokemije. V sklopu diplomske naloge smo vzorce bakrovih metanoatov najprej sintetizirali, kasneje pa smo jih analizirali s pomočjo rentgenske praškovne difrakcije (XRD) in termogravimetrične analize (TGA). Našo predpostavljeno hipotezo smo potrdili, saj nam je uspelo sintetizirati različne modifikacije bakrovih metanoatov s spreminjanjem parametrov, kot so volumen in koncentracija mravljične kisline ter masa bazičnega bakrovega karbonata, ki sta služili kot vstopni spojini. Sonochemistry is the field od chemistry, where chemical reactions take place under the infulence of sound energy, called ultrasound. It deals with understanding of the effect of sound waves in chemical systems. The aim of our study was to synthesize various modifications of copper methanoates using not only classical methods but also methods of sonochemistry. Within the thesis, samples of copper methanoates were first synthesized and subsequently analysed using X-ray powder diffraction (XRD) and thermogravimetric analysis (TGA). Our assumed hypothesis was confirmed, because we have managed to synthesize various modifications of copper methanoates by varying parameters such as volume and concentration of formic acid as well as mass of basic copper carbonate, which were used as the input compounds. baker koordinacijske spojine bakrovi metanoati sonokemija rentgenska praškovna difrakcija termogravimetrična analiza copper coordination compounds copper formates sonochemistry X-ray powder diffraction thermogravimetric analysis true true false [M. Biškop] Slovenski jezik Angleški jezik Diplomsko delo/naloga 2015-08-20 14:16:08 2015-10-30 09:56:51 2022-06-04 03:10:32 2021-05-09 03:32:24 2015 0 Maribor 0 0000-00-00 NiDoloceno NiDoloceno NiDoloceno 0000-00-00 0000-00-00 0000-00-00 544.57(043.2) 19428374 URN:SI:UM:DK:TJ9M0I5A UN_Biskop_Mateja_2015.pdf UN_Biskop_Mateja_2015.pdf 1 75DF4CA1200FCE44D65074863D4767A5 5d722c0ee844e22f4da906f0fcf13e18bd6b9fc389e2efc71e536c4161d5ccfe ab4b6600-7c07-11eb-bb7a-00155d0001ca https://dk.um.si/Dokument.php?lang=slv&id=79118 Fakulteta za kemijo in kemijsko tehnologijo 0 0 0