20.500.12556/DKUM-77485 Vpliv strukture tiola na polimerizacije v koloidnih medijih diplomsko delo univerzitetnega študijskega programa I. stopnje The effect of the thiol structure on the polymerisation in colloidal media Namen diplomskega dela je bilo ugotovit, kako struktura tiola vpliva na polimerizacijo v koloidnih medijih. Pripravili smo multilplo emulzijo (V/O/V), kjer je bil delež vodne faze večji od 80 %. Sintetizirane kroglice smo prefiltrirali skozi filterpapir in jih očistili z metanolom, nato je sledila karakterizacija teh kroglic. Kroglice smo pripravili s kombinacijo TMPTMP/TMPTA in TT/TMPTA ter 1,6-HDT/TMPTA. Sintetizirane kroglice smo slikali z mikroskopom in jim izmerili velikost ter tako določili povprečno velikost sintetizirane kroglice in velikostno porazdelitev v vzorcu. Prav tako smo jih okarakterizirali z elementno analizo in s FTIR. The purpuse od this thesis was to determine how the structure of thiol affects the polymerisation in colloidal media. We prepared a multiple emulsion (V/O/V), where the proportion of VF was greater that 80 %. The synthesized grains were filtered through filter paper and purified with methanol, followed by characterization of these grains. The grains were prepared with combination of TMPTMP/TMPTA, TT/TMPTA and 1,6-HDT/TMPTA. The synthesized grains were imaged with microscope and measured to detremine the averagce size of synthesized porous grains and the size distribution of the grains in the sample. We aswell did the EA and FTIR. poliHIPE tiol-en polimerizacija suspenzijska polimerizacija porozna zrna polyHIPE thiol-ene suspension polymerisation porous beads true true false [N. Ozis] Slovenski jezik Angleški jezik Diplomsko delo/naloga 2020-09-01 13:29:59 2020-10-21 08:20:37 2022-08-09 15:37:29 2023-12-18 03:32:51 2020 0 Maribor 0 Maribor [X], 33 str. 0000-00-00 NiDoloceno NiDoloceno NiDoloceno 0000-00-00 0000-00-00 0000-00-00 66.095.26:544.773(043.2) 33436419 URN:SI:UM:DK:WBL0EQQP UN_Ozis_Nika_2020.pdf UN_Ozis_Nika_2020.pdf 1 2850C282F7CF54DCBD9A1B6D0A569AA1 aa2bbccd47fa0e0ddefeaa4d161608e3a81b4e7278d5ca9af4ef213eb27e6e93 53fa7ea5-7c04-11eb-bb7a-00155d0001ca 20.500.12556/dkum/8cfcb200-7d1d-4904-ab17-5df8f61afad9 https://dk.um.si/Dokument.php?lang=slv&id=145112 Fakulteta za kemijo in kemijsko tehnologijo 0 0 0