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Title:Characterization of defects in PVD TiAlN hard coatings
Authors:ID Gselman, Peter (Author)
ID Bončina, Tonica (Author)
ID Zupanič, Franc (Author)
ID Panjan, Peter (Author)
ID Kek-Merl, Darja (Author)
ID Čekada, Miha (Author)
Files:.pdf Materiali_in_Tehnologije_2012_Gselman_et_al._CHARACTERIZATION_OF_DEFECTS_IN_PVD_TiAlN_HARD_COATINGS.pdf (716,32 KB)
MD5: 81B30479F191C688AE6B4ADA887C533E
 
URL http://mit.imt.si/Revija/izvodi/mit124/gselman.pdf
 
Language:English
Work type:Scientific work
Typology:1.01 - Original Scientific Article
Organization:FS - Faculty of Mechanical Engineering
Abstract:PVD hard coatings are continuously gaining their importance in different fields of applications. In industrial use, they are often exposed to corrosive environments. Hard coatings possess inherently good corrosion resistance, but the substrate-hard coating systems may suffer from a severe corrosion attack due to the defects (craters, pin holes) in the coatings. On the sites, where defects extend through the coating, pitting corrosion can take place. These sites are drawbacks in the applications of hard coating. A PVD TiAlN hard coating was prepared on cold-work, tool-steel (AISI D2) substrates by sputtering using unbalanced magnetron sources. The growth defects incorporated into the coating were studied after the deposition and corrosion experiments. We used two methods: (1) scanning electron microscopy (SEM) for general overview of the coating topography and 2D-characterization of defects, and (2) scanning electron microscopy with a focused ion beam (SEM-FIB) for making serial cross-sections through the selected defects in order to provide images for a 3D-reconstruction of defects. In this work we tried to investigate the formation of a defect at a specific location and findout whether the selected defect causes pitting corrosion.
Keywords:trde prevleke, PVD prevleke, defekti, jamičasta korozija, mikrostruktura, PVD hard coating, defect, pitting corrosion, microstructure
Publication status:Published
Publication version:Version of Record
Year of publishing:2012
Number of pages:str. 351-354
Numbering:Letn. 46, št. 4
PID:20.500.12556/DKUM-50133 New window
ISSN:1580-2949
UDC:621.793:669.058.67:66.019
ISSN on article:1580-2949
COBISS.SI-ID:16153622 New window
NUK URN:URN:SI:UM:DK:ZMEF31CI
Publication date in DKUM:10.07.2015
Views:1593
Downloads:110
Metadata:XML DC-XML DC-RDF
Categories:Misc.
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Record is a part of a journal

Title:Materiali in tehnologije
Shortened title:Mater. tehnol.
Publisher:Inštitut za kovinske materiale in tehnologije
ISSN:1580-2949
COBISS.SI-ID:106193664 New window

Document is financed by a project

Funder:ARRS - Slovenian Research Agency
Project number:L2-2100
Name:Razvoj nove generacije trdih prevlek s pulznim naprševanjem

Secondary language

Language:Slovenian
Title:Karakterizacija defektov PVD TiAlN trdih prevlek
Abstract:PVD trde prevleke pridobivajo pomen na različnih področjih uporabe. Pri različnih aplikacijah so pogosto izpostavljene korozijskemu okolju. Trde prevleke so kemijsko inertne in same po sebi korozijsko obstojne. Med njihovo pripravo pa nastane v njih veliko defektov (kraterji, "pinholi"). Nekateri od njih segajo do podlage. Na teh mestih pride do jamičaste korozije, kar pa je z vidika uporabe neželeno. TiAlN-prevleko smo nanesli na podlago orodnega jekla D2 po postopku naprševanja z neuravnoteženim magnetronskim izvirom. Defekte, ki so nastali med pripravo plasti, smo preučili po korozijskem preizkusu. Za analizo smo uporabili dve metodi. Vrstični elektronski mikroskop(SEM), s katerim smo pridobili splošni pregled prevleke, kot tudi 2D-karakterizacijo defektov. Kot drugo metodo smo uporabili fokusiran ionski curek, ki je integriran v klasični SEM, s katerim smo izvedli serijo rezov izbranih defektov za njihovo 3D-karakterizacijo. V delu smo poskušali na specifičnih mestih ugotoviti mehanizem nastanka defektov in ugotovljali, ali povzročajo jamičasto korozijo.
Keywords:PVD hard coating, defect, 3D-reconstruction, FIB, SEM


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