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Title:Extraction of lutein diesters from tagetes erecta using supercritical $CO_2$ and liquid propane
Authors:ID Škerget, Mojca (Author)
ID Bezjak, Miran (Author)
ID Makovšek, Katja (Author)
ID Knez, Željko (Author)
Files:.pdf Acta_Chimica_Slovenica_2010_Skerget_et_al._Extraction_of_lutein_diesters_from_Tagetes_erecta_using_supercritical_CO2_and_liquid_propane.pdf (156,17 KB)
MD5: CA880181CF9A625800BF1CCB81ABBD12
 
URL http://acta-arhiv.chem-soc.si/57/57-1-060.pdf
 
Language:English
Work type:Scientific work
Typology:1.01 - Original Scientific Article
Organization:FKKT - Faculty of Chemistry and Chemical Engineering
Abstract:The efficiency of high pressure extraction of lutein diesters from marigold (Tagetes erecta) flower petals has been investigated. The solvents used for extraction were supercritical carbon dioxide and liquid propane. Operating parameters were 300 bar and 40, 60 and 80 °C for $CO_2$ and 100, 150, 200 bar and 40 and 60 °C for propane, respectively. The influence of process parameterson the total yield of extraction and content of lutein diesters in the extracts was investigated. The results show, that solvent power of propanefor lutein diesters is approximately 3.5 times higher than of $CO_2$. The calculation procedure based on the Fick's second law was applied to determine the diffusivities of lutein diesters during extraction from marigold flower petals for both extraction stages: a constant rate stage followed by a stage of decreasing rate. The mathematical model based on the Fick's second law well described the experimental extraction results.
Keywords:lutein diesters, Tagetes errecta, extraction, supercritical $CO_2$, subcritical propane
Publication status:Published
Publication version:Version of Record
Year of publishing:2010
Number of pages:str. 60-65
Numbering:Letn. 57, št. 1
PID:20.500.12556/DKUM-52378 New window
ISSN:1318-0207
UDC:664.87.061-987
ISSN on article:1318-0207
COBISS.SI-ID:14011158 New window
NUK URN:URN:SI:UM:DK:O0YMMPWX
Publication date in DKUM:10.07.2015
Views:1661
Downloads:161
Metadata:XML DC-XML DC-RDF
Categories:Misc.
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Record is a part of a journal

Title:Acta Chimica Slovenica
Shortened title:Acta Chim. Slov.
Publisher:Slovensko kemijsko društvo
ISSN:1318-0207
COBISS.SI-ID:14086149 New window

Document is financed by a project

Funder:ARRS - Slovenian Research Agency
Project number:P2-0046
Name:Separacijski procesi in produktna tehnika

Licences

License:CC BY 4.0, Creative Commons Attribution 4.0 International
Link:http://creativecommons.org/licenses/by/4.0/
Description:This is the standard Creative Commons license that gives others maximum freedom to do what they want with the work as long as they credit the author.
Licensing start date:10.07.2015

Secondary language

Language:Slovenian
Abstract:Raziskali smo učinkovitost visokotlačne ekstrakcije diestrov luteina iz cvetov žametnice (Tagetes erecta). Topila, ki smo jih uporabili za ekstrakcijo so bila superkritični ogljikov dioksid in tekoči propan. Obratovalni parametri so bili tlak 300 bar in temperatura 40, 60 in 80 °C v primeru $CO_2$ ter 100, 150 in 200 bar in 40 in 60°C za propan. Raziskali smo vpliv obratovalnih parametrov na izkoristek ekstrakcije in vsebnost luteinskih diestrov v ekstraktih. Rezultati so pokazali da je propan boljše topilo za diestre luteina kot $CO_2$, njegova topnostna moč je približno 3,5 krat višja od $CO_2$. Difuzivnost luteinskih diestrov med ekstrakcijo cvetov žametnice smo izračunali z uporabo modela, ki temelji na 2. Fickovem zakonu in sicer za dve stopnji ekstrakcije: stopnjo konstantne ekstrakcijske hitrosti, ki ji sledi stopnja padajoče ekstrakcijske hitrosti. Matematični model na osnovi 2. Fickovega zakona je dobro opisal eksperimentalne ekstrakcijske podatke.
Keywords:diestri luteina, Tagetes erecta, ekstrakcija, superkritični $CO_2$, subkritični propan


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