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Title:
Synthesis and structure of hydroxylammonium fluorosilicates
Authors:
ID
Kristl, Matjaž
(
Author
)
ID
Drofenik, Mihael
(
Author
)
ID
Golič, Ljubo
(
Author
)
Files:
http://www.dlib.si/details/URN:NBN:SI:doc-F80CU1M7
Language:
Slovenian
Work type:
Not categorized
Typology:
1.01 - Original Scientific Article
Organization:
FKKT - Faculty of Chemistry and Chemical Engineering
Abstract:
A new hydroxylammonium compound with the formula ▫$(NH_3OH)_2SiF_6$▫ has been synthesized by reaction of solid ▫$NH_3OHF$▫ and ▫$H2SiF6$▫. By recrystallization fromaqueous HF, single-crystals of ▫$(NH_3OH)_2Si_F6.2H_2O$▫ were isolated. Both compounds were characterized by elemental analysis and thermal analysis, the structure of ▫$(NH_3OH)_2SiF_6.2H_2O$▫ has been determined by single crystal x-ray analysis. The compound crystallizes monoclinic.
Keywords:
anorganska kemija
,
fluorosilikati
,
hidroksilamini
,
sintetiziranje spojin
Publisher:
Slovensko kemijsko društvo
Year of publishing:
2002
Number of pages:
str. 243-250
Numbering:
Vol 49, 2
PID:
20.500.12556/DKUM-53118
UDC:
546
ISSN on article:
1318-0207
COBISS.SI-ID:
7169046
NUK URN:
URN:SI:UM:DK:K4SIH9HU
Publication date in DKUM:
10.07.2015
Views:
1530
Downloads:
59
Metadata:
Categories:
Misc.
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Record is a part of a journal
Title:
Acta Chimica Slovenica
Shortened title:
Acta Chim. Slov.
Publisher:
Slovensko kemijsko društvo
ISSN:
1318-0207
COBISS.SI-ID:
14086149
Secondary language
Language:
Slovenian
Title:
Sinteza in struktura hidroksilamonijevih fluorosilikatov
Abstract:
Z reakcijo med trdnim ▫$NH_3OHF$▫ in raztopino ▫$H_2SiF_6$▫ smo sintetizirali novo spojino hidroksilamina s formulo ▫$(NH_3OH)_2SiF_6$▫. Pri rekristalizaciji te spojine iz vodne raztopine HF smo izločili monokristale s sestavo ▫$(NH_3OH)_2SiF_6.2H_2O$▫ Obe spojini smo karakterizirali s kemijsko in termično analizo, strukturo ▫$(NH_3OH)_2SiF_6.2H_2O$▫ smo določili z rentgensko strukturno analiza na osnovi monokristala. Spojina kristalizira monoklinsko.
Keywords:
inorganic chemistry
,
fluorosilicates
,
hydroxylammonium compound
,
synthesis
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