| Title: | Synthesis of Au nanoparticles prepared with ultrasonic spray pyrolysis and hydrogen reduction |
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| Authors: | ID Stopić, Srečko (Author) ID Rudolf, Rebeka (Author) ID Bogovic, Jelena (Author) ID Majerič, Peter (Author) ID Čolić, Miodrag (Author) ID Tomić, Sergej (Author) ID Jenko, Monika (Author) ID Friedrich, Bernd (Author) |
| Files: | Materiali_in_tehnologije_2013_Stopic_et_al._Synthesis_of_Au_Nanoparticles_Prepared_With_Ultrasonic_Spray_Pyrolysis_and_Hydrogen_Reductio.pdf (3,17 MB) MD5: 91DE512173CD3CBCBB627B8F4C977E34
http://mit.imt.si/Revija/izvodi/mit135/stopic.pdf
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| Language: | English |
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| Work type: | Scientific work |
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| Typology: | 1.01 - Original Scientific Article |
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| Organization: | FS - Faculty of Mechanical Engineering
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| Abstract: | Golden nanoparticles of different sizes and shapes (spherical, cylindrical, triangular and round) where prepared during a synthesis of gold with ultrasonic spray pyrolysis (USP) and hydrogen reduction. The experimental investigations of the (USP) method were performed with an ultrasonic source of 0.8 MHz and 2.5 MHz, acting on the water solution of HAuCl4 forming aerosols with micron-sized and nanosized droplets. The results of the investigation show that the final shape and size of the Au particles depend on the characteristics of the solution and the frequency of the ultrasound. The second step of synthesizing the Au nanoparticles includes the subsequent thermal decomposition of the aerosol droplets in a hydrogen atmosphere between 260°C and 500°C. The investigations showed that the Au nanoparticles prepared in this way are smaller and more homogeneous. |
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| Keywords: | gold, ultrasonic spray pyrolysis, reduction, nanoparticles |
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| Publication status: | Published |
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| Publication version: | Version of Record |
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| Year of publishing: | 2013 |
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| Number of pages: | str. 577-583 |
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| Numbering: | Letn. 47, št. 5 |
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| PID: | 20.500.12556/DKUM-56263  |
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| ISSN: | 1580-2949 |
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| UDC: | 669.21:620.3:66.017 |
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| ISSN on article: | 1580-2949 |
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| COBISS.SI-ID: | 17274390  |
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| NUK URN: | URN:SI:UM:DK:AMKJOBJ5 |
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| Publication date in DKUM: | 21.12.2015 |
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| Views: | 2014 |
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| Downloads: | 134 |
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| Metadata: |  |
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| Categories: | Misc.
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