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Title:Synthesis of Au nanoparticles prepared with ultrasonic spray pyrolysis and hydrogen reduction
Authors:ID Stopić, Srečko (Author)
ID Rudolf, Rebeka (Author)
ID Bogovic, Jelena (Author)
ID Majerič, Peter (Author)
ID Čolić, Miodrag (Author)
ID Tomić, Sergej (Author)
ID Jenko, Monika (Author)
ID Friedrich, Bernd (Author)
Files:.pdf Materiali_in_tehnologije_2013_Stopic_et_al._Synthesis_of_Au_Nanoparticles_Prepared_With_Ultrasonic_Spray_Pyrolysis_and_Hydrogen_Reductio.pdf (3,17 MB)
MD5: 91DE512173CD3CBCBB627B8F4C977E34
 
URL http://mit.imt.si/Revija/izvodi/mit135/stopic.pdf
 
Language:English
Work type:Scientific work
Typology:1.01 - Original Scientific Article
Organization:FS - Faculty of Mechanical Engineering
Abstract:Golden nanoparticles of different sizes and shapes (spherical, cylindrical, triangular and round) where prepared during a synthesis of gold with ultrasonic spray pyrolysis (USP) and hydrogen reduction. The experimental investigations of the (USP) method were performed with an ultrasonic source of 0.8 MHz and 2.5 MHz, acting on the water solution of HAuCl4 forming aerosols with micron-sized and nanosized droplets. The results of the investigation show that the final shape and size of the Au particles depend on the characteristics of the solution and the frequency of the ultrasound. The second step of synthesizing the Au nanoparticles includes the subsequent thermal decomposition of the aerosol droplets in a hydrogen atmosphere between 260°C and 500°C. The investigations showed that the Au nanoparticles prepared in this way are smaller and more homogeneous.
Keywords:gold, ultrasonic spray pyrolysis, reduction, nanoparticles
Publication status:Published
Publication version:Version of Record
Year of publishing:2013
Number of pages:str. 577-583
Numbering:Letn. 47, št. 5
PID:20.500.12556/DKUM-56263 New window
ISSN:1580-2949
UDC:669.21:620.3:66.017
ISSN on article:1580-2949
COBISS.SI-ID:17274390 New window
NUK URN:URN:SI:UM:DK:AMKJOBJ5
Publication date in DKUM:21.12.2015
Views:2014
Downloads:134
Metadata:XML DC-XML DC-RDF
Categories:Misc.
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Record is a part of a journal

Title:Materiali in tehnologije
Shortened title:Mater. tehnol.
Publisher:Inštitut za kovinske materiale in tehnologije
ISSN:1580-2949
COBISS.SI-ID:106193664 New window

Document is financed by a project

Funder:ARRS - Slovenian Research Agency
Project number:L2-4212
Name:Tehnologija izdelave Au nano-delcev

Secondary language

Language:Slovenian
Title:Sinteza Au-nanodelcev, pripravljenih z ultrazvočno razpršilno pirolizo in redukcijo z vodikom
Abstract:Zlate nanodelce različnih velikosti in oblik (sferični, cilindrični, trikotni in okrogli) smo pripravili s sintezo zlata z uporabo ultrazvočne razpršilne pirolize (USP) in redukcije. Eksperimentalne raziskave USP-metode so bile izvedene z ultrazvočnim izvirom s frekvenco med 0,8 MHz in 2,5 MHz z delovanjem na vodno raztopino HAuCl4, kjer je prišlo do formiranja aerosolov z mikro- in nanovelikostjo kapljic. Rezultati preiskav kažejo, da je oblika in velikost nastalih Au-delcev odvisna od karakteristik raztopine in od frekvence ultrazvoka. Drugi proces sinteze Au-nanodelcev je vključeval kasnejšo toplotno dekompozicijo kapljic aerosola. Izveden je bil v vodikovi atmosferi med 260°C in 500°C. Preiskave so pokazale, da so tako izdelani Au-delci bolj homogeni in manjši.
Keywords:zlato, ultrazvočna razpršilna piroliza, redukcija, nanodelci


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