| Title: | DSC/TG of Al-based alloyed powders for p/m applications |
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| Authors: | ID Šuštaršič, Borivoj (Author)
ID Medved, Jože (Author)
ID Glodež, Srečko (Author)
ID Šori, Marko (Author)
ID Korošec, Albert (Author)
ID Inštitut za kovinske materiale in tehnologije (Copyright holder) |
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| Files: |  Materiali_in_Tehnologije_2014_Sustarsic_et_al._DSCTG_OF_Al-BASED_ALLOYED_POWDERS_FOR_PM_APPLICATIONS.pdf (319,52 KB)
MD5: 66FE70852AB300A099894C5B32E83963
 http://mit.imt.si/Revija/izvodi/mit144/sustarsic.pdf
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| Language: | English |
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| Work type: | Scientific work |
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| Typology: | 1.01 - Original Scientific Article |
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| Organization: | FNM - Faculty of Natural Sciences and Mathematics
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| Abstract: | Al-based alloyed powders, appropriate for the sintering procedure (powder metallurgy, P/M) contain the alloying elements with a high solid solubility in Al, enabling reaction and liquid-phase sintering. They are surface oxidised because of a high affinity of Al to oxygen. Besides, this type of powders contains a polymeric lubricant (wax), which reduces the friction on die walls during automatic die compaction into the final compact shape of a product. This lubricant has to be removed slowly during the first stage of sintering in order to prevent deformations and cracking of the product. Consequently, its sintering is very complex. Generally, these powders are sintered in pure nitrogen with a low dew point. The optimum sintering conditions are generally determined on the basis of light and scanning electron microscopy. The investigation can also be completed very successively with differential scanning calorimetry and thermo gravimetry. The first one allows an insight into the endo- and exothermic reactions, taking place during the heating and cooling of a compacted metal powder, and the second one allows an insight into the processes, connected with the mass loss (a reduction, a lubricant removal, etc.) or mass increase (an oxidation). The DSC/TG of three commercial Al-based alloyed powders was performed in the frame of our investigations. The results were compared with the theoretical thermodynamic-based calculations and the optimum sintering conditions were proposed. |
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| Keywords: | aluminium powders, sintering, differential scanning calorimetry and thermo gravimetry |
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| Publication status: | Published |
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| Publication version: | Version of Record |
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| Submitted for review: | 13.11.2013 |
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| Article acceptance date: | 16.04.2014 |
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| Publisher: | Institute of Metals and Technology |
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| Year of publishing: | 2014 |
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| Number of pages: | 5 str. |
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| Numbering: | Letn. 48, št. 4 |
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| PID: | 20.500.12556/DKUM-65178  |
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| ISSN: | 1580-2949 |
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| UDC: | 621.762.5:669.71 |
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| ISSN on article: | 1580-2949 |
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| COBISS.SI-ID: | 18068246 |
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| NUK URN: | URN:SI:UM:DK:LVTZOKOK |
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| Publication date in DKUM: | 15.03.2017 |
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| Views: | 1508 |
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| Downloads: | 151 |
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| Metadata: |    |
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| Categories: | Misc.
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