| Title: | Synthesis comparison and characterization of chitosan-coated magnetic nanoparticles prepared with different methods |
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| Authors: | ID Hojnik Podrepšek, Gordana (Author)
ID Knez, Željko (Author)
ID Leitgeb, Maja (Author)
ID Inštitut za kovinske materiale in tehnologije (Copyright holder) |
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| Files: |  Materiali_in_Tehnologije_2014_Podrepsek,_Knez,_Leitgeb_Synthesis_Comparison_and_Characterization_of_Chitosan-Coated_Magnetic_Nanoparticl.pdf (1022,83 KB)
MD5: 303FA0933B4C81E3B2D2D728AAFA316A
 http://mit.imt.si/Revija/izvodi/mit145/hojnik.pdf
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| Language: | English |
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| Work type: | Scientific work |
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| Typology: | 1.01 - Original Scientific Article |
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| Organization: | FKKT - Faculty of Chemistry and Chemical Engineering
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| Abstract: | In this study, magnetic maghemite nanoparticles were prepared with the coprecipitation method, due to its simplicity and productivity. Thereafter, chitosan-coated magnetic nanoparticles were synthesized with three different methods, the micro-emulsion process, the suspension cross-linking technique and the covalent binding. Subsequently, a comparison of the used methods was done using various analyses such as Fourier transform infrared spectroscopy (FTIR), scanning electron microscopy (SEM), thermogravimetry (TGA), differential scanning calorimetry (DSC), vibrating-sample magnetometry (VSM) and dynamic light scattering (DLS). The characterization results from Fourier transform infrared (FTIR) spectroscopy and thermogravimetric analysis (TGA) indicated a successful binding of chitosan on the magnetic nanoparticles. SEM pictures showed that spherical structured particles with an increased particle size were obtained as the chitosan layer around the particles was increased. Considering that the magnetic-separation technique has the advantages of rapidity, high efficiency, cost-effectiveness and lack of negative effect on the biological activity, these carriers may be applied in enzyme immobilization. |
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| Keywords: | magnetic nanoparticles, chitosan, surface functionalization |
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| Publication status: | Published |
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| Publication version: | Version of Record |
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| Year of publishing: | 2014 |
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| Number of pages: | str. 689-692 |
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| Numbering: | Letn. 48, št. 5 |
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| PID: | 20.500.12556/DKUM-65239  |
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| ISSN: | 1580-2949 |
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| UDC: | 66.02 |
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| ISSN on article: | 1580-2949 |
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| COBISS.SI-ID: | 18207766 |
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| NUK URN: | URN:SI:UM:DK:LI4JOXO6 |
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| Publication date in DKUM: | 23.03.2017 |
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| Views: | 1849 |
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| Downloads: | 127 |
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| Metadata: |    |
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| Categories: | Misc.
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