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Title:Solvotermalna sinteza zeolitnih nanokompozitov
Authors:ID Zanjkovič, Neža (Author)
ID Kristl, Matjaž (Mentor) More about this mentor... New window
ID Stergar, Janja (Comentor)
ID Nemet, Andreja (Comentor)
Files:.pdf MAG_Zanjkovic_Neza_2026.pdf (5,20 MB)
MD5: 1FE630F0C0D7646E686C4A9B5CE50E55
 
Language:Slovenian
Work type:Master's thesis/paper
Typology:2.09 - Master's Thesis
Organization:FKKT - Faculty of Chemistry and Chemical Engineering
Abstract:Zeolitni nanokompoziti so zaradi adsorpcijskih sposobnosti zeolitov in magnetnih lastnosti železovih oksidov obetavni materiali pri uporabi v katalizi, pri sanaciji okolja in dostavi zdravil. V sklopu magistrske naloge smo najprej s soobarjanjem in z modularnim pretočnim mikroreaktorskim sistemom sintetizirali magnetne nanodelce, ki smo jih uporabili pri hidrotermalni sintezi zeolitnih nanokompozitov. Zeolitne nanokompozite smo sintetizirali tudi s soobarjanjem železovih soli v prisotnosti zeolita. Poleg različnih sinteznih tehnik smo spreminjali razmerja med zeolitom in magnetnimi nanodelci. Učinkovitost sintez in lastnosti vzorcev smo preverili z vibracijskim magnetometrom, z dinamičnim sipanjem svetlobe, s Fourierjevo transformacijsko infrardečo spektroskopijo, s termogravimetrično analizo in z vrstično elektronsko mikroskopijo.
Keywords:soobarjanje, modularni pretočni mikroreaktorski sistem, hidrotermalna sinteza, magnetni nanodelci, zeolitni nanokompoziti
Place of publishing:Maribor
Year of publishing:2026
PID:20.500.12556/DKUM-99558 New window
Publication date in DKUM:10.09.2026
Views:101
Downloads:16
Metadata:XML DC-XML DC-RDF
Categories:KTFMB - FKKT
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Licences

License:CC BY-NC-ND 4.0, Creative Commons Attribution-NonCommercial-NoDerivatives 4.0 International
Link:http://creativecommons.org/licenses/by-nc-nd/4.0/
Description:The most restrictive Creative Commons license. This only allows people to download and share the work for no commercial gain and for no other purposes.
Licensing start date:19.08.2026

Secondary language

Language:English
Title:Solvothermal synthesis of zeolite nanocomposites
Abstract:Zeolite nanocomposites are promising materials for applications in catalysis, environmental remediation, and drug delivery due to the adsorption capabilities of zeolites and the magnetic properties of iron oxides. In this work, we first synthesized magnetic nanoparticles via co-precipitation and a modular flow microreactor system. The resulting nanoparticles were subsequently used in the hydrothermal synthesis of zeolite nanocomposites. We also synthesized zeolite nanocomposites by co-precipitation of iron salts in the presence of zeolite. In addition to various synthesis techniques, we varied the ratios of zeolite to magnetic nanoparticles. We evaluated the efficiency of the synthesis and the properties of the samples using a vibrating sample magnetometer, dynamic light scattering, Fourier transform infrared spectroscopy, thermogravimetric analysis and scanning electron microscopy.
Keywords:co-precipitation, modular flow microreactor system, hydrothermal synthesis, magnetic nanoparticles, zeolite nanocomposites


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